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Synthesis And Characterisation Of Lead Suphide Semiconductor Nanostructures Using Chemical Bath Deposition Method – Complete project material

CHAPTER ONE 1.0                                           INTRODUCTION 1.1 BACKGROUND OF THE RESEARCH Nanocrystalline semiconductors have been the subject of intense research 1 due to their unique physical and chemical properties2,3. Evidence shows that reducing the particle (grain) size of…

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Synthesis And Biological Activities Of Phenylsulphonylaminoalkanamides – Complete project material

ABSTRACT   Palladium catalysed synthesis of substituted 2-[acetyl(phenylsulphonyl)amino]-3-methylbutanamide (176) is reported. The intermediate 2-[acetyl(phenylsulphonyl)amino]-3-methybutanamide (175) was obtained by the reaction between 2-[acetyl(phenylsulphonyl)amino]-3-methybutanoic acid chloride (175) and ammonia. Substituted 2-[acetyl (phenylsulphonyl)amino]-3-methylbutanamides (176a-f) were obtained by coupling2-[acetyl…

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Synthesis And Application Of Azo-Anthraquinone Disperse Dyes On Polylactide Fabrics. – Complete project material

ABSTRACT   The synthesis of some disperse dyes base on anthraquinone was achieved by coupling diazotised 1-aminoanthraquinone and tetrazotised 1,4-diaminoanthraquinone respectively with pyridone derivatives. The identity of the resultant dyes were investigated using UV-visiblespectrophotometry, Fourier…

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Syntheses, Characterization And Antimicrobial Activities Of Alkynylated Angular Phenoxazines And Alkynylated Naphthoquinones – Complete project material

ABSTRACT The synthesis of ten new alkynylated derivatives of angular phenoxazine and alkynylatednaphthoquinone was thoroughly investigated. The first intermediate, 6-chloro-5Hbenzo[a]phenoxazin-5-one was obtained by the condensation of 2-aminophenol with 2,3-dichloro-1,4- naphthoquinone in the presence of anhydrous…

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Syntheses Of Benzothiazinophenothiazine Derivatives And Evaluation Of Their Antimicrobial Activities – Complete project material

ABSTRACT   The syntheses of benzothiazinophenothiazine derivatives from simple heterocyclic compounds asprecursors is described. Condensation of 2-aminothiophenol with 2,3-dichloro-1,4-naphthoquinone inan alkaline medium furnished a good yield of the intermediate, 6-chloro-5H-benzo[a]phenothiazin-5-one. Further condensation of the intermediate…

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Studies In The Deproteinization Potential Of Coconut Water (Cocos Nucifera) Natural Rubber Latex – Complete project material

ABSTRACT The use of untreated natural rubber latex for the production of dipped goods has suffered a major setback due to numerous complaints of allergy traced to inherent protein content, a number of conventional treatment…

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Spectrophotometric Determination Of Vanadium(Iii) And Vanadium(V) Using 2-[(E)-[3-[(E)-(2-Hydroxyphenyl)Methyleneamino] Phenyl]Iminomethyl]Phenol – Complete project material

ABSTRACT 2-[(E)-[3-[(E)-(2-hydroxyphenyl)methyleneamino]phenyl]iminomethyl]phenol was synthesized from the condensation reaction of 1,3-diaminobenzene and 2-hydroxyzaldehyde in dimethylformaldehyde (DMF). Its coordination characteristic with vanadium(III) and vanadium(V) complexes was studied via, UV/Visible, IR and NMR spectroscopy; stoichiometric, melting point and…

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Spectrophotometric Determination Of Niacin, Thiamine, Glibenclamide, Erythromycin And Para Amino Benzo Ic Acid Using 2, 3 – Dichloro – 5, 6 – Dicyano – 1, 4 – Benzoquinone – Complete project material

ABSTRACT A simple and sensitive spectrophotometric method is described for the assay of thedrugs; niacin, glibenclamide, erythromycin, thiamine and 4-aminobenzoic acid. Themethod is based on charge transfer complexation (CT) reaction of niacin, glibenclamide,erythromycin, thiamine and…

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Concentration Of Cadmium, Lead And Chromium In Human Whole Blood – Complete project material

ABSTRACT Human whole blood samples obtained from blood banks in different hospitals inEnugu State were analyzed for cadmium, lead and chromium concentrationsusing atomic absorption spectrophotometric method. The results of the analysisshowed that about 72.7% of…

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Comparative Assessment Of Performance Of Aluminium Sulphate (Alum) And Ferrous Sulphate As Coagulants In Water Treatment – Complete project material

ABSTRACT Aluminium Sulphate (Alum) and ferrous sulphate, being among the best known coagulants in water treatment were investigated with the aim of comparing their coagulation efficiencies. The parameter levels of a turbid water were determined…

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